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논문 기본 정보

자료유형
학술저널
저자정보
L. H. Bac (University of Ulsan) B. K. Kim (University of Ulsan) J. S. Kim (University of Ulsan) J. C. Kim (University of Ulsan)
저널정보
한국자기학회 Journal of Magnetics Journal of Magnetics Vol.16 No.4
발행연도
2011.12
수록면
435 - 439 (5page)

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초록· 키워드

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In this work, we prepared Fe-Ni alloy nanopowders by wire electrical explosion in deionized water and ethanol. Particles size and morphology of the as-synthesized nanoparticles prepared in water and ethanol were observed by transmission electron microscopy. In both cases, the as-synthesized nanoparticles were in nearly spherical shape and their size distribution was broad. The particles prepared in the water were in core-shell structure due to the oxidation of Fe element. X-ray diffraction was used to analyze the phase of the nanopowders. It showed that the nanopowders prepared in water had γ-Fe-Ni solid solution and FeO phase. The samples obtained in ethanol were in two phases of Fe-Ni solid solution, γ-Fe-Ni and α-Fe-Ni. Bulk samples were made from the as-synthesized nanopowders by spark plasma sintering at 1000 oC for 10 min. Structure of the bulk sample was observed by scanning electron microscope. Magnetic properties of the as-synthesized nanopowders and the bulk samples were investigated by vibrating sample magnetometer. The hysteresis loop of the assynthesized nanopowders and the sintered bulk samples revealed a ferromagnetic characteristic.

목차

1. Introduction
2. Experimental
3. Results and Discussion
4. Conclusion
References

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UCI(KEPA) : I410-ECN-0101-2013-428-001369125