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연구자들이 자신의 연구와 전문성을 널리 알리고, 새로운 협력의 기회를 만들 수 있는 네트워킹 공간이에요.
초록· 키워드
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Separation of basic compounds using reverse phase chromatography on a silica-based stationary phase represents a major challenge, because of the interaction between the cationic sites of the basic compounds with the anionic silanols of the stationary phase. This study presents a simple, reliable, and organic solvent - free liquid chromatographic method for the determination of terbutaline and salbutamol, in which a room temperature ionic liquid (RTIL) is used as mobile phase additive. We investigated various mobile phase parameters affecting the retention of the two compounds, such as types and concentration of RTILs and, pH of the mobile phase were investigated. The developed method was validated according to International Conference on Harmonization (ICH) guidelines and successfully applied effectively to determine salbutamol sulfate in pharmaceutical preparations.
목차
Abstract
1. Introduction
2. Experimental
3. Results and Discussion
4. Conclusions
References
참고문헌 (20)
참고문헌 신청
Y. Gaber, U. Tornvall, M. A. Kumar, M. A. Amin and R. Hatti- Kaul, Green Chem., 13, 2021-2025 (2011).
A. Rios and M. Zougagh, Trends Anal. Chem., 43, 174-188 (2013).
F. T. G. van den Brink, W. Olthuis, A. van den Berg and M. Odijk, Trends Anal. Chem., 70, 40-49 (2015).
F. Pena-Pereira, I. Lavilla and C. Bendicho, Trends Anal. Chem., 29, 617-628 (2010).
H. M. Mohamed, Trends Anal. Chem., 66, 176-192 (2015).
A. Rios and M. Zougagh, Trends Anal. Chem., 43, 174-188 (2013).
F. T. G. van den Brink, W. Olthuis, A. van den Berg and M. Odijk, Trends Anal. Chem., 70, 40-49 (2015).
F. Pena-Pereira, I. Lavilla and C. Bendicho, Trends Anal. Chem., 29, 617-628 (2010).
H. M. Mohamed, Trends Anal. Chem., 66, 176-192 (2015).
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UCI(KEPA) : I410-ECN-0101-2020-433-001079935