지원사업
학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
커뮤니티
연구자들이 자신의 연구와 전문성을 널리 알리고, 새로운 협력의 기회를 만들 수 있는 네트워킹 공간이에요.
논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 저널정보
- 한국농약과학회 농약과학회지 농약과학회지 제24권 제4호
- 발행연도
- 2020.12
- 수록면
- 321 - 333 (13page)
- DOI
- 10.7585/kjps.2020.24.4.321
이용수
초록· 키워드
오류제보하기
In the present study, an analytical method was developed and optimized for screening and confirmation of multi-pesticide residues in farmed aquatic animal samples. Target pesticides (organochlorines, organophosphorus, and synthetic pyrethroids) were extracted via the QuEChERS (quick, easy, cheap, effective, rugged, and safe) approach. Ethyl acetate was used for extraction of pesticides from the samples (flatfish, eel, shrimp, and Manila clam), which were then purified using C<SUB>18</SUB> and primary secondary amine. Finally, the extracts were filtered through a 0.22-μm polytetrafluoroethylene syringe filter and subsequently analyzed using gas chromatography coupled with mass spectrometry. The target analytes were ionized in the positive mode of electron impact ionization using multiple reaction monitoring. According to the CODEX CAC/GL-71 guideline, accuracy, precision, linearity, and limit of detection were evaluated for all matrices. The accuracy (recoveries) was between 62.4% and 120%, and precision (relative standard deviations) was below 20%. The linearity of the matrix calibration curves was r²>0.98. The limits of detection and quantification for all pesticides were ≤3 μg/kg and ≤10 μg/kg, respectively. In real sample (n=79) analysis, trifluralin was detected at 67 μg/kg in one Manila clam sample. Based on our results, the proposed method was satisfactory for pesticide residue determination in aquatic animal products.
목차
Abstract
Introduction
Materials and Methods
Results and Discussion
Conclusions
Literature Cited
참고문헌 (30)
참고문헌 신청
Antonious GF / 2012 / On-farm bioremediation of dimethazone and trifluralin residues in runoff water from an agricultural field / Journal of Environmental Science and Health-Part B Pesticides, Food Contaminants, and Agricultural Wastes 47(7):608~621
Bondad-Reantaso MG / 2005 / Disease and health management in Asian aquaculture / Veterinary Parasitology 132(3-4 SPEC):249~272
Codex Alimentarius Commission / Guidelines for the design and implementation of national regulatory food safety assurance programme associated with the use of veterinary drugs in food producing animals CAC/GL 71
Cao Y / 2015 / A novel method based on MSPD for simultaneous determination of 16 pesticide residues in tea by LC-MS/MS / Journal of Chromatography B:Analytical Technologies in the Biomedical and Life Sciences :998~999
Chan D / 2012 / Detection of the illegal use of Trifluralin in shrimp farming. Residues of Veterinary Drugs in Food / Proceedings of the EuroResidue VII Conference 1:429~433
Bondad-Reantaso MG / 2005 / Disease and health management in Asian aquaculture / Veterinary Parasitology 132(3-4 SPEC):249~272
Codex Alimentarius Commission / Guidelines for the design and implementation of national regulatory food safety assurance programme associated with the use of veterinary drugs in food producing animals CAC/GL 71
Cao Y / 2015 / A novel method based on MSPD for simultaneous determination of 16 pesticide residues in tea by LC-MS/MS / Journal of Chromatography B:Analytical Technologies in the Biomedical and Life Sciences :998~999
Chan D / 2012 / Detection of the illegal use of Trifluralin in shrimp farming. Residues of Veterinary Drugs in Food / Proceedings of the EuroResidue VII Conference 1:429~433
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