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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 저널정보
- 한국전기전자재료학회 Transactions on Electrical and Electronic Materials Transactions on Electrical and Electronic Materials 제22권 제6호
- 발행연도
- 2021.12
- 수록면
- 843 - 850 (8page)
- DOI
- https://doi.org/10.1007/s42341-021-00309-0
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초록· 키워드
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The carbonization performance of the iron-containing carbon film resulting from polyimide was examined, Polyimide/Fe composite films were prepared from Iron (III) 2,4-pentanedionate (Fe(acac)) and poly(amic acid) (PAA) based on ODA and PMDA via a solution process in DMAC, followed by carbonization the polyimide film at a temperature range of 600?1600 °C. The organized polyimide/Fe combined fi lms were characterized using a scanning electron microscope (SEM), and thermogravimetric analysis (TGA), X-ray diffraction (XRD), and Raman. The formation of Fe particles and the synthesis of polyimide (PMDA/ODA) in the polyimide matrix is confirmed by FTIR results. Meantime, in the polyimide matrix, Fe particles were well spread which were showed by the SEM images. Kinetic parameters and thermal stability of the degradation methods for the organized polyimide/Fe combined films were examined in N 2 environment by TGA. The results have shown that the values of the calculated activation energies and thermal stability increased of the (Fe (acac)) the activation energy and loading also different with the weight-loss rate for all compositions.
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참고문헌 (28)
참고문헌 신청
F. E. Elbakoush / 2017 / Carbonization behavior of polyimide fi lms hybrid with different metal catalyst / Polym. Sci., Ser. B 59(4):430~436
H. Gajiwala / 1998 / Hybridized resin matrix approach applied for development of carbon/carbon composites—I / Carbon 36(7?8):903~912
D. Zhong / 2005 / Graphitization behavior of the boron-containing carbon fi lm derived from polyimide / NAOSITE 35(64):63~67
Y. Hishiyama / 1988 / Structure and properties of highly crystallized graphite fi lms based on polyimide Kapton / J. Mater. Sci 23(9):3272~3277
D. Zhong / 2000 / A study of fi lm thickness dependence of the graphitizability of PMDA–ODA polyimide-derived carbon fi lm / Carbon 38(15):2161~2165
H. Gajiwala / 1998 / Hybridized resin matrix approach applied for development of carbon/carbon composites—I / Carbon 36(7?8):903~912
D. Zhong / 2005 / Graphitization behavior of the boron-containing carbon fi lm derived from polyimide / NAOSITE 35(64):63~67
Y. Hishiyama / 1988 / Structure and properties of highly crystallized graphite fi lms based on polyimide Kapton / J. Mater. Sci 23(9):3272~3277
D. Zhong / 2000 / A study of fi lm thickness dependence of the graphitizability of PMDA–ODA polyimide-derived carbon fi lm / Carbon 38(15):2161~2165
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