Hydrogen has been considered as an attractive alternative to fossil fuels particularly over the past decade and is considered by many a barbinger to the hydrogen economy. Hydrogen can be produced using divers, domesitc resources-including fossil fuels such as natural gas and coal. 90% of the world’s hydrogen is currently obtained by the reformation of fossil fuels, which consumes much energy and is accompanied by serious CO2 emissions. Electrolysis is a promising option for hydrogen production from renewable resoruces. Electrolysis is the process of using electricity to split water into hydrgen and oxygen. PEM electrolysis allows higher current density and safety advantages such as lack of corrosive electrolyte. The acid environment used to the catalysts such as Pt group metal(PGM), resulting in high cost. Alkaline electrolysis enables the attractive operating parameter becuase alkaline electrolysis applied non-precious metal or oxides as electrolcatalysts. While alkaline electrolysis materials are still less stable and efficient than PEM materials. PEM electrolysis requires a high amount of costly PGM catalysts, and liquid alkaline electrolysis is not well suited for intermittent operation. Uusing the anion exchagne membrane water electrolysis cells(AEMWEC) method expedcted result in high efficiency. The anodic and cathodic half cells are separated by an AEM, in the presence of middle alkaline electrolyte solution circulating only through the anodic half-cell. The PGM electrocatalyst indicated a higher activity and stability. It is necessary to develope inexpensive non-precious metal electrocatalysts such as metal oxdie, perovskite and layered double hydroxide. In this study, we were synthesized 0D & 1D CuCoO catalyst and performace activity for Oxygen evolution reaction. CoCoO NP was synthesized using a Co-precipitaion method. And, 1D CuCoO NP was synthesized by electrospinning. The morphologies and structures of CuCoCo nano materials were characterized by FE-SEM, and XRD, XPS, BET. The activity of the OER catalyst was analysis with LSV. In this case, it can be seen as an cuurent density, tafel-plot, overpotentail, onset potential. And the stability test to investigate the durability was performed. This test was progressed in static potential 1.85V vs. NHE in 1M KOH for 5h