메뉴 건너뛰기
.. 내서재 .. 알림
소속 기관/학교 인증
인증하면 논문, 학술자료 등을  무료로 열람할 수 있어요.
한국대학교, 누리자동차, 시립도서관 등 나의 기관을 확인해보세요
(국내 대학 90% 이상 구독 중)
로그인 회원가입 고객센터 ENG
주제분류

추천
검색

논문 기본 정보

자료유형
학위논문
저자정보

민은수 (안동대학교, 안동대학교 일반대학원)

지도교수
신형섭
발행연도
2023
저작권
안동대학교 논문은 저작권에 의해 보호받습니다.

이용수11

표지
AI에게 요청하기
추천
검색

이 논문의 연구 히스토리 (4)

초록· 키워드

오류제보하기
The hydrogen embrittlement evaluation of metallic materials is important to secure safety in the hydrogen production, transportation, and storage processes. The slow strain tensile test (SSRT) is a generally adopted test method for evaluating hydrogen embrittlement in a high-pressure hydrogen environment. It uses an autoclave to perform the test. However, high cost is required due to advanced facility operation and strict safety protocols. Therefore, it is necessary to develop a simple and fast but reliable test method for screening the hydrogen embrittlement compatibility of carbon steels for storage containers and transportation pipelines. The small punch (SP) test method is more convenient than other test methods, which enables a quantitative evaluation of hydrogen embrittlement compatibility of steels in an external hydrogen environment, such as an actual high-pressure hydrogen storage tank and pipelines. From the viewpoint of establishing a reliable but simple test method, it is important to compare it with the SSRT, which corresponds to the standard test method for screening the hydrogen embrittlement compatibility of steel. Therefore, in this study, to establish a hydrogen embrittlement sensitivity evaluation technique in a high-pressure hydrogen environment and to improve reliability, the SP test and SSRT were used for two kinds of pipeline steels of API X70 and X52 steels to comparatively evaluate the hydrogen embrittlement behavior during each test method. For the SSRT, a hollow tensile specimen was used instead of the conventional autoclave pressure vessel. In particular, it is necessary to compare and evaluate with the SSRT to understand the reduction phenomenon of the maximum load on the load-displacement curves during SP tests due to their characteristic hydrogen embrittlement behavior of ferritic steels. The effect of hydrogen embrittlement through the SSRT under a high-pressure hydrogen environment differed from the results of SP tests which showed a decrease in the maximum load when hydrogen embrittlement occurred. Moreover, according to the results obtained by SSRT using hollow tensile specimen, the hydrogen embrittlement occurred at the non-uniform plastic deformation region (usually corresponds to the necking region) after UTS, which leads to rapid fracture, indicating a decrease in elongation. In addition, the effect of hydrogen embrittlement induced in high-pressure hydrogen environments was investigated by observing the SEM fractography of fractured specimens after the SP test and the SSRT. They supported the behaviors of the load-displacement curves or the stress-strain curves obtained.

목차

목 차 i
List of Figures iii
List of Tables vii
제 1 장 서 론 1
1.1 연구 배경 1
1.2 수소에너지 세계 동향 2
1.3 수소에너지 국내 동향 4
1.4 수소취화 거동 시험법 6
1.5 연구 목적 및 내용 9
제 2 장 시험방법 11
2.1 시험편 11
2.2 In-situ SP 시험방법 14
2.3 중공인장시험편 사용 in-situ SSRT 시험방법 19
2.4 수소취화 민감도의 정량 평가 23
제 3 장 시험결과 및 고찰 28
3.1 In-situ SP 시험결과: 배관강의 수소취화 민감도 정성 평가 28
3.1.1 API X70강 28
3.1.2 API X52강 36
3.2 In-situ SSRT 시험결과: 배관강의 수소취화 민감도 정성 평가 44
3.2.1 API X70강 44
3.2.2 API X52강 56
3.3 배관강의 수소취화 민감도 정량 평가 63
3.3.1 API X70강 63
3.3.2 API X52강 71
3.4 중도정지 SSRT 중공인장시험편의 단면관찰을 통한 수소취화 거동 파악 78
제 4 장 결론 및 향후 계획 88
4.1 결론 88
4.2 향후 계획 89
참고문헌 91
Abstract 95
감사의 글 97

최근 본 자료

전체보기

댓글(0)

0