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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2017.3
- 수록면
- 77 - 81 (5page)
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The aim of this study was to investigate a validation method for determination of tricin in Phragmites communis ears. Tricin was isolated with chromatographic methods and used as the standard substances for quantitative analysis. The structural determination was characterized by comparing their NMR spectral data with values reported in the literature. For validation, the specificity, linearity, precision, accuracy, detection limits, and quantification limits of tricin was measured by HPLC. The results show that the specificity was satisfied with retention time and diode array detector (DAD) spectrum by analysis of tricin using HPLC. The limits of detection (LOD) for tricin was 0.84 mg/ml. Recovery of tricin was 98.80~108.22% with R.S.D values less than 2%. Intra-day and inter-day precisions of tricin in P. communis ears were 99.96~100.96% and 99.01~100.40%, respectively. Therefore, application of tricin was validated by an analytical method as major compound in P. communis ears.
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참고문헌 (14)
참고문헌 신청
Baxter, H. / 1999 / The Handbook of Natural Flavonoids / John wiley & Sons
Martens, S. / 2005 / Flavones and flavone synthases / Phytochemistry 66:2399~2407
Lu, B. / 2005 / Toxicology and safety of anti-oxidant of bamboo leaves. Part 1: Acute and subchronic toxicity studies on anti-oxidant of bamboo leaves / Food Chem. Toxicol 43:783~792
Verschoyle, R. D. / 2006 / Preliminary safety evaluation of the putative cancer chemopreventive agent tricin, a naturally occurring flavone / Cancer Chemother. Pharmacol 57:1~6
Chang, C. L. / 2010 / Quiquelignan A-H, eight new lignoids from the rattan palm Calamus quiquesetinervius and their antiradical, anti-inflammatory and antiplatelet aggregation activities / Bioorg. Med. Chem 18:518~525
Martens, S. / 2005 / Flavones and flavone synthases / Phytochemistry 66:2399~2407
Lu, B. / 2005 / Toxicology and safety of anti-oxidant of bamboo leaves. Part 1: Acute and subchronic toxicity studies on anti-oxidant of bamboo leaves / Food Chem. Toxicol 43:783~792
Verschoyle, R. D. / 2006 / Preliminary safety evaluation of the putative cancer chemopreventive agent tricin, a naturally occurring flavone / Cancer Chemother. Pharmacol 57:1~6
Chang, C. L. / 2010 / Quiquelignan A-H, eight new lignoids from the rattan palm Calamus quiquesetinervius and their antiradical, anti-inflammatory and antiplatelet aggregation activities / Bioorg. Med. Chem 18:518~525
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